Fully automatic reaction system
The Fully Automatic High-Pressure Intelligent Reaction System is an independently developed and designed fully automatic six-station robotic reaction device by Laibei Instruments. It is mainly designed for chemical reactions in corrosive and high-risk environments. It can cooperate with robotic arms to perform automatic feeding, temperature rising, cleaning, discharging and other operations without manual intervention throughout the process.
Multi-axis robotic arm with precise material level recognition, capable of gripping test tubes, flipping and pouring materials, and four/six-station cruise feeding. The entire system can achieve fully automatic operations, including automatic feeding of solid and liquid materials, multi-mode cleaning (ordinary cleaning, acid cleaning, heating flushing, multiple cycle cleaning), automatic discharging, lifting and opening/closing fixation of the reaction chamber, pressure relief and gas release;
High-precision intelligent touch screen controller capable of displaying the temperature inside the cover/heater (jacket oil temperature), stirring speed display and setting, measurement and display of the pressure inside the reactor, as well as overpressure automatic venting release protection, automatic gas release, automatic cleaning, automatic lifting, automatic opening/closing, and automatic data collection.
It has intelligent temperature control without temperature surge, and the temperature control is accurate. The heating rate is adjustable. There is an acousto - optic alarm for over - temperature and over - pressure, and it can automatically cut off the heating power supply. Multiple mis - operation alarm prompts are set during the operation to ensure the safe and smooth progress of the entire experimental process. There is no leakage, and no exposed rotating parts, making the experiment safer.
15-inch industrial-grade touch screen with digital temperature display; imported components, Hastelloy anti-corrosion safety explosion-proof membrane, no welding inside the components, stable structure, and can be moved as a whole. Smooth operation, high torque, no sparks, long service life.
Freely adjustable touch screen angle, human-machine interaction, friendly interface; local area network, Ethernet, APP remote control, etc.
Can provide customized equipment for specific experiments according to different configuration requirements of customers.
| Item | Details |
|---|---|
| Main Configuration | Multi-axis robotic arm (collaborative robot), hydrothermal reaction chamber x4/6, temperature control device (electric heating furnace/oil bath machine), micro high-precision intelligent touch screen controller, feeding pump x4/6, cleaning meter (pump), automatic operation mechanism and switching actuator, supporting frame (integral floor-standing chassis) |
| Number of Stations | 4/6 |
| Sealing Method | Flexible gasket sealing, snap-ring quick-opening fastening, snap-ring automatic opening and closing without manual operation |
| Volume | 50/100/250 mL, cylindrical |
| Hydrothermal Reactor Head Configuration | Pressure gauge, pressure sensor, explosion-proof membrane, temperature thermocouple, intake valve, vent valve, stirring head, N2 replacement, vacuum pumping, liquid sampling valve (optional) |
| Maximum Operating Temperature | 250/300℃ |
| Maximum Operating Pressure | 10/20MPa |
| Temperature Control Method | Electric heating jacket temperature control, accuracy ≤0.3℃, PID program temperature control, heating power 0 - 100% stepless adjustable |
| Stirring Method | Mechanical stirring, beveled mixing stirring head (suitable for hydrothermal reaction) or customized |
| Data Acquisition | Can automatically collect temperature, pressure, rotation speed, etc. of each station |
| Inner Diameter/Inner Height | 50/100/250mL corresponding to 36/65, 36/115, 61/96 mm |
| Robotic Arm | Multi-claw/joint design, load: 3 - 5kg, torque: 70 - 120N.cm, rotation speed: 50 - 1500 rpm adjustable, the robotic arm is suspended on the chassis along the track for cruise movement to accurately identify targets, realizing sliding, grasping, flipping, pouring, and resetting (4 - 6 stations) |
| Controller Functions | High-precision intelligent touch screen controller, temperature inside the reactor/heater (jacket oil temperature), stirring speed display and setting, measurement and display of the pressure inside the reactor, intake/N2 replacement/vacuum pumping, overpressure automatic venting release protection, automatic gas release, automatic cleaning, automatic lifting, automatic opening/closing, over-temperature and over-pressure sound and light alarm automatic power cutoff, automatic data collection, program remote controllable (independently developed software) |
| Independent Switches | One-button emergency stop switch, independent heating switch, main switch |
| Material | 316L stainless steel, Hastelloy C276 and HB, titanium, zirconium..., alloy materials can improve acid and alkali corrosion resistance, high temperature and high pressure resistance |
| Feeding - Discharging - Cleaning | Fully automated process without manual intervention, specifically including automatic feeding of solid and liquid materials, multi-mode cleaning (ordinary cleaning, acid cleaning, heating flushing, multiple cycle cleaning), automatic discharging, lifting and opening/closing fixation of the reaction chamber, pressure relief and gas release |
| High Precision Processing | Hydrothermal reaction chamber is integrally formed without welding points throughout, and all components have no welding points |
| Dimensions | 4 stations: WxDxH 1450x750x1800 mm, 6 stations: WxDxH 2000x750x1800 mm |
| Electrical Details | Independent dual 220V or 380V, 50/60Hz |
| Overall Power | ≤5500W |
| Weight | Approximately 200kg |
a. All materials used in Laibei Instruments' equipment meet international standards.
b. Laibei Instruments has passed the ISO 9001 Enterprise Quality Management System Certification, ISO 14001 Environmental Management System Certification, ISO45001 Occupational Health and Safety Management System Certification, and CE Certification.
c. All production materials used by Laibei Instruments comply with the RoHS standard to ensure environmental protection and the health of users.
The R&D team of Laibei Instruments' reaction kettles comes from international brand reaction kettle manufacturing companies. With years of experience in importing reaction kettles and considering the needs of domestic users, they have independently developed and designed more than 40 types of reaction kettles with a volume range from 25mL to 20L, a temperature range from -40℃ to 700℃, and a pressure range from high vacuum to 40MPa.
Laibei Instruments independently develops and designs core-competitive instruments and equipment mainly including reaction kettles, reaction system integration devices, and sample pretreatment equipment, which are widely used in scientific research fields such as petrochemical, materials metallurgy, biopharmaceuticals, energy and environment. All equipment can be customized according to customer needs.
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